Fully Automatic Glove Box ZKYQX-I Gas Purification and Recirculation System

Fully Automatic Glove Box ZKYQX-I Gas Purification and Circulation System

One. Glove Box Function

Sealed Recirculation

The inert gas within the glove box is circulated and purified through a closed loop by a recirculating fan and purifier, continuously removing moisture and oxygen.

Automatic Control Regeneration

Deoxygenation materials can be regenerated, with the regeneration process controlled by a program.

Cabinet Pressure Control

The glove box's internal pressure is automatically controlled by a PLC. The working pressure can be freely set within +/- 1500Pa, and the system automatically protects against deviations beyond +/- 1500Pa.

Vacuum pump automatic control

Vacuum pumps are required to automatically activate when needed in the system.

II. Main Components and Configurations

Integrated with a sealed housing (including a sloped operating surface safety glass one-way vision window), transition compartment, recirculation purification unit, PLC control and touch screen operating system, vacuum system, display system, bracket (integral) etc.

Basic Configuration

1 stainless steel 304 cabinet

One large transition compartment made of stainless steel

1 mini transition cabin

1 pair of butyl rubber gloves

1 lighting system

1 piece per box power interface

4 KF40 spare interfaces

1 high-performance recirculating fan, 90 m³/h capacity

1 vacuum pump

1 set of water probe

1 Oxygen Probe Set

Stool casters

Foot switch

III. Technical Specifications:

Water Oxygen Index: Less than 0.1 ppm.

2. Leak Rate: ＜0.001 vol%/h

3. Technical Specifications

1). Glove box housing

(1) Case: 304 stainless steel, thickness 3mm

(2) Inner surface: Stainless steel; Outer surface: Powder coated, white

(3) Studio Size: 1220mm x 760mm x 900mm (L x W x H)

(4) Dimensions: 1935mm x 790mm x 1800mm (Length x Width x Height)

(5) Front Window: Inclined view window, 8mm thick transparent tempered safety glass, coated with anti-corrosion film, wear-resistant, corrosion-resistant, and good light transmission.

(6) Glove Mouth: Made of anodized aluminum, sealed with an O-ring, diameter 220mm

(7) Gloves: Butyl rubber, thickness 0.4mm, diameter 8", length 32"

(8) Filter: 0.3 micron specification, 1 gas inlet and 1 gas outlet

(9) Shelves: Made of stainless steel, adjustable height.

(10) Cabinet Lighting: LED lights, installed above each glass window in front

(11) Interface: 4 spare interfaces, DN 40 KF material: SUS304 stainless steel; chuck-type quick assembly interface, allowing gas or liquid to enter the box safely and conveniently.

(12) Power Interface: 1 (220V) located inside the glove box work compartment, providing power to electrical equipment. A power strip is installed inside the glove box, featuring three sets of outlets with both two-prong and three-prong options.

(13) Foot switch: Controls the gas replenishment and evacuation of the housing, located below the housing, for fine-tuning the pressure inside the work chamber.

(14) Glove Box Frame: Carbon steel with electrostatic powder coating, one-piece design; equipped with swivel casters and adjustable support legs; portable glove box.

(15) Vacuum Gauge: Mechanical dial display, measures vacuum levels in overpressure and tool overpressure chambers, WIKA Germany.

4. Large Transition Hatch

On the right side of the housing; diameter 385mm x 600mm, material: SUS304 stainless steel;

Airtightness: Leakage rate ≤ 0.001 Vol%/h.

(1) Attachment

Slide Trays: 304 Stainless Steel

Hatch: Double door, anodized aluminum material, thickness 10mm, vertical operation, equipped with a pressure gauge with analog display

(2) Control

Electromagnetic Valve Touchscreen Automatic Operation

5. Small transition compartment

Size: Diameter 150mm, Length 300mm, Length into the housing 100mm

Material: 304 Stainless Steel

Surface: Inner surface with brushed finish, outer surface painted (white)

(1) Attachment

Hatch: Double doors, pressure-latch opening method Pressure gauge: Analog display

(2) Control

Manual Valve - Manual Operation

6. Gas Purification and Recirculation System

Purification Column

Function: Gas-tight, moisture and oxygen removal (recirculation capacity 90 m³/h)

Container Material: 304 Stainless Steel

Purification Materials: Copper Catalyst: 4kg; Molecular Sieve: 6kg

Purification Capacity: Oxygen Removal: 60L; Water Removal: 2Kg

Water Oxygen Index: Less than 0.1ppm (empty box)

(2) Circulatory System

Working Gases: Nitrogen, Argon

Recirculation Capacity: Integrated Fan Flow Rate 90 m³/h

(3) Recycled

Operation: PLC automated control of regeneration process

Argon Gas: working gas mixed with H2 (5-10% H2)

(4) Vacuum Pump

Spec: 12m3/h, scroll pump, with oil mist filter, air vibration control

Valve

Main Valve: DN 40 KF, Electromagnetic Angle Valve

Control Valve: Electromagnetic Integrated Valve

7. Control System

Function: Includes self-diagnosis, power-off self-start feature, with pressure control and adaptive functions; automatic control, cycle control, password protection; unit control with Siemens PLC touch screen.

Pressure Control: The pressure in the housing and transition compartment can be freely set within +/- 1500 Pa working pressure, with automatic protection activated beyond +/- 1500 Pa.

Foot pedal: Controls the pressure inside the cabinet, facilitating the operation of increasing and decreasing pressure.

Display System: Utilizes Siemens PLC touch screen PT177 to show operational status, cabinet pressure, system records, etc.

8. Vacuum System Control Status

Vacuum Pump - Flow rate: 8 m³/h, Ultimate Vacuum: ≤2x10^-1 Pa. Can be started manually or via PLC, suitable for vacuuming transition chambers and maintaining cabinet pressure balance. Ultimate Vacuum: ≤2x10^-1 Pa.

9. Oxygen probe

Imported Brand AII from the USA, featuring ±0.1ppm high precision, electrochemical sensor, 0-1000PPM display values, and low drift.

10. Water Probe

Imported Vaisala (Finland), measurement range: 0-1000PPM with clear readings, low drift, wide application, especially for lithium battery manufacturing and metal-organic users. Can be restored to initial state through cleaning and regeneration process, avoiding the issue of one-time contamination leading to disposal.

Water and Oxygen Indices: Measurement data from the water and oxygen analyzers must be displayed, and an alarm must sound if values exceed the set limits.

11. Acceptance Criteria

Under standard conditions, at a standard atmospheric pressure, using a 99.999% pure inert gas source, and with the container running empty, the water oxygen content is less than 0.1 ppm, and the container leakage rate is ≤0.001 Vol%/h.